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CORE SERVICE OFFERINGS

Chemical Testing

TCR has a state-of-the-art chemical analysis laboratory with expert chemists. It has the capability to analyze ferrous and non-ferrous metals, ceramics, glass, refractories, mineral and Ferro alloys in PPB or PPM level or in percentage. TCR’s capabilities include: Wet Chemistry, Optical Emission Spectroscopy(OES), Inductively Coupled Plasma(ICP) Spectrometer, Automatic Combustion based Carbon and Sulfur determinator, Glow Discharge spectrometer for (GDS) chemical depth profiling, and more.

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Testing and Inpsections using XRF alloy analyzers in Multiple Industry Verticals in India - Metals, Electronics, Soils, Mining, Minerals, Woods, Thin Films, Paints & Coatings, Oils & Liquids, and Hazardous Waste Materials. XRF, India, Lead, Pb, testing, inspection, Paint, soil, metals, RoHS, WEEE, EPA, Mining. TCR Engineering Services, an India based material testing and quality assurance company undertakes tests using X-Ray Florescence (XRF) portable alloy analyzers on Metals, Electronics, Soils, Mining, Minerals, Woods, Thin Films, Paints & Coatings, Oils & Liquids, and Hazardous Waste Materials. The Material Testing Laboratory at TCR Engineering Services in India have devised testing programs to help clients understand the rigorous RoHS restrictions. TCR has acquired specialized equipment and researched the complex methodologies required to test for the compliance.

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CHEMICAL

TESTING

An inherent strength of TCR Engineering Services is the ability to successfully undertake analytical chemistry assignments. The highly qualified analytical chemists are experienced in using the full range of analytical instruments including state-of-the-art Spectrometers and Wet Chemistry laboratory facilities. TCR caters to all analytical requirements for Ferrous, Non-Ferrous Metals, Ceramics, Glass, Refractory, Minerals and Ferro Alloys. The chemical department analyzes samples in all forms including drillings or turnings, solid samples, and liquids.

 

 

The Classical Wet Chemistry (bench chemistry) Department uses Gravimetry (chemical species is determined by weighing) and Titrimetry (involves volume measurement of a liquid reactant) procedures to analyze the chemical composition of materials. It assists in the identification of unknown materials and gaining an understanding of their chemical composition, structure and function. Most classical wet chemical methods can accommodate comparatively small amounts of a sample in diverse shapes or forms. Fully compliant with the environmental standards of India, the wet chemistry department at TCR is highly sought-after by leading companies all over the world, right form trace chemical analysis to very low detection levels. 
 

Chemical Testing

TECHNICAL CAPABILITIES

TCR has an extensive list of accredited testing capabilities

TCR Engineering Material Testing Laboratory provides both analytical and interpretive expertise, including method development, method validation and identification of unknown materials. The lab can successfully meet all challenges, whether it is for PPB or PPM level analysis or in percentage. TCR has the capability to provide results with both, standard specifications and client supplied specifications. It has the expertise to develop customized analytical procedures for analysis of materials and substances for which no protocol is available.

​Chemical Analysis by Classical Wet Method

  1. Ferrous Metals (Including) C, S, P, Mn, Cr, Mo, Ni

  2. Non-Ferrous Refractory, Ceramics, and Minerals, Ferro Alloys (Fe-Mn, Fe-Si, Fe-Mn-Si, Fe-Mg-Si, Low C Fe-Cr, Fe-Mo)

  3. Non-Ferrous Metals (Each Additional Element)

  4. Elements Such As Co, Al, W, Cu, Sn, Ti, Mg, V In Steel

  5. Nitrogen / Boron / Palladium (Each Element)

  6. Purity Of Cu

  7. Purity Of Al, Zn, Pb, Ni, Bi, Cd, Sn, Mg, W, Ti 

  8. Oxygen Analysis and Hydrogen Analysis

 

Chemical Analysis by Spectrometers

  1. EDAX Analysis

  2. Complete Chemical Analysis up to 8 elements

  3. Impurities in PPM Level using AAS or ICP

 

Chemical Analysis by LECO

  1. Oxygen by LECO

  2. Nitrogen by LECO

  3. Hydrogen by LECO

Steel and Cast Iron

  1. Determination Of Any One Element (%C)

  2. Determination Of Any One Element (Mn, Si)

  3. Determination Of Any One Element (Ni, Cr, S, 

  4. Determination Of C, Mn, Si, S, P
    Complete Analysis Of Low Alloy Steel Up To 8 Elements Including C, S, P, Si, Mn, Ni, Cr, Mo

  5. Determination Of Any One Element in Stainless Steel 

  6. Complete Analysis Of Stainless Steel up to 8 Elements

  7. Determination Of High Alloy Element (Cr, Ni, Mn)

  8. Determination Of Some Special Element  (Cu, Ti, Co, V, W, Al) Per Element

  9. Complete Analysis Of High-Speed Steel (8 Elements) Per Element

  10. Determination Of Mo%

  11. Determination Of V%

  12. Nitrogen In Steel

 

Non-Ferrous Material

  1. Copper Base Alloys

  2. Determination Of Any One Element

  3. Complete Analysis Of 6 Elements

  4. Purity Test Of Cu

  5. Purity Test Of Other Non-Ferrous Element 

 

Ferro Alloys

  1. Analysis of Main Element

  2. Each Subsequent Element

Tin, Aluminum, Lead Base

  1. Determination of Any One Element

  2. Complete Analysis of up to 8 Elements

  3. Purity Test

  4. Only Aluminum %

 

Other Tests

  1. pH Value Determination
    Sand Content (as Sio2)

  2. Acid Insoluble
    Sulphates, Chlorides, Silicates, Carbonates, Oxides of Iron Per Element

  3. Elemental analysis – Calcium, Magnesium, Potassium, Sodium, Iron Per Element

  4. Moisture Content

  5. Analysis on XRF per element

  6. Ash Content

  7. Material Certification

  8. Unknown Material Identification

  9. Trace Element Analysis

  10. Oil, Powdered Metal, & Chips/Shavings Analysis

  11. Solder Alloys (Tin/Lead)

  12. Quantitative and Semi-Quantitative Analyses

  13. Density of Powdered Metals

  14. Plating and Plating Solution Analysis
    Glass Analysis

  15. On-Site Positive Material Identification (PMI)

  16. Coating Identification

  17. Coating Weights

  18. Particle Size Analyzer

EQUIPMENT

Wet Chemistry

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  1. Microwave Oven System

 

2. Electro Analyzers (4 Nos.)​

 

3. Electronic Balances (3 Nos.)

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4. Vacuum Pump, Muffle Furnaces and Heating Ovens and more.

Spectrometer: 

Atomic Absorption (AA) Graphite Furnace Spectrometer

The sensitivity of GFAA enables performances of elemental analysis that is virtually impossible using other analytical techniques. These are used to determine ppm and sub-ppm levels of residuals in metals. GFAA is also particularly useful for the determination of low boiling point tramp elements in aerospace alloys. This method is particularly pertinent in material analysis for the detection of trace metals.


Inductively Coupled Plasma Spectrometer

ICP is a spectrophotometric method carried out in solutions where high temperature argon plasma is used to reduce matrix effects, giving straight-line calibrations. This enables low sample weights to be analyzed and coupled with its wide calibration range making them the most flexible instruments that are available today with parts per billion detection limits. 


Optical Emission Spectrometer

These instruments enable the rapid quantitative determination of a wide range of alloys including carbon/low alloy steels, stainless steels, cast irons, aluminum alloys, nickel alloys and copper alloys. It entails a relatively simple sample preparation that allows a rapid turnaround of results using this technique.

 

X-Ray Diffraction Spectrometer

X-Ray Diffraction Analysis (XRD) investigates the crystalline material structure, including atomic arrangement, crystallite size, and imperfections. The X-rays are generated by a cathode ray tube, filtered to produce monochromatic radiation, collimated to concentrate, and directed toward the sample.
 

Combustion carbon and sulphur determination are accepted as the most accurate methods for determining carbon and sulphur in metal, ore or powder samples. These samples may be in the form of solid material, drillings or powders. This technique is mainly used to complement ICP or OES for a full chemical analysis of metallic samples.
 

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TCR Engineering has a wide range of equipment that is available for chemical analysis: 

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OIL ANALYSIS

FERROGRAPHY

Ferrography or oil analysis, is a series of laboratory tests that determine the condition of used lubricants in equipment components, over a period of time. A trend of Wear Particle distribution and their concentration typically presents the condition of the equipment. It allows organizations to be proactive as it provides them with the opportunity to be prepared for investing in maintenance programs for breakdowns.

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There are six basic Wear Particle types generated through the wear process, which includes metallic particles that comprise of Normal Rubbing Wear, Cutting Wear Particles, Spherical Particles, Severe Sliding Particles, Bearing Wear Particles (Fatigue Spall Particles, Laminar Particles) and Gear Wear (Pitch Line Fatigue Particles, Scuffing or Scoring Particles).  Sand and dirt particles responsible for generating Wear Particles exist in the system too. 
 

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Reduction in Unscheduled Downtime due to Wear of Rotary Components like Bearings and Gears 

Effective Maintenance Scheduling 

Improved Equipment Reliability and Safety 

Reduction in Maintenance Costs 

Maximization of Oil Change-out Intervals that Indirectly Conserves Environmental Cleanliness 

Reduction in Machine Power Consumption Over a Period of Time

Oil Analysis Ferrography

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RoHS Compliance Testing

RoHS Compliance Testing

The RoHS Directive states that certain non-exempt products, as well as electrical and electronic products available in the market within the EU, must contain less than 0.1% lead (Pb), mercury (Hg), hexavalent chromium (Cr6+), polybrominated biphenyls (PBB), and polybrominated diphenyl ethers (PBDE), and less than 0.01% cadmium (Cd). Product manufacturers including computer hardware, IT equipment, clock radios and toasters could find themselves banned from selling their product in the European market if they fail to comply with the new directives.

 

TCR Engineering Services has devised testing programs to help clients understand the rigorous RoHS restrictions. TCR has researched complex methodologies required for compliance testing and has acquired specialized equipment to meet client needs. The RoHS Testing Team at TCR has the capability to analyze all restricted substances up to the required limits and they ensure that the products meet all the requirements while retaining full product functionality.

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  1. Restriction of (certain) Hazardous Substances (RoHS) is a result of Waste Electronic and Electrical Equipment (WEEE) Directive, which addresses end-of-life issues on electrical components
     

  2. The WEEE Directive is essentially concerned with the introduction of hazardous materials into the environment, during recycling or disposal

Lead Inspection

TCR CORE CAPABILITY:

The RoHS Testing Team at TCR analyses concentrations of lead, mercury, cadmium, chromium, polybrominated biphenyls (PBBs), and polybrominated diphenyl ethers (PBDEs) in electrical and electronic components, right up to the required limits, to ensure that all the products meet the requirements while retaining their full functionality. TCR Engineering Services undertakes RoHS and WEEE-related compliance testing for electronic products and accessories using both:

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Non Destructive RoHS screening (RFA method)

The screening provides indications about the presence of hazardous substances in the product according to RoHS. It is best suited to gain a quick overview of a goods receipt check or in preliminary inspections. Using a custom-tailored portable X-Ray Fluorescence Spectroscopy (XRF) spectrometer, the inspection team from TCR can simultaneously screen for all five restricted RoHS elements and chlorine (Cl), in a matter of a few seconds. Using a Portable XRF is non-destructive and an in-situ point-and-shoot screening method for PVC, PE, alloys, metals, solders, ceramics and packaging materials.  

 

Chemical Analysis by ICP (Verification method)
RoHS testing is carried out using an initial screening test by XRF; if high levels of restricted substances are found, additional tests may be performed using Inductively Coupled Plasma (ICP) Spectrometer and wet chemistry. The Chemical Analysis Department at TCR provides all its clients with accurate, precise results that report the total level of RoHS elements and compounds, along with detailed information about their products meeting all RoHS requirements.

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Lead Inspection and Detection

The ill-effects of Lead (Pb) consumption is gaining significance all over the world. The Lead inspection service from TCR allows manufacturers of consumer electronics materials, children's toys and jewelry, cooking or edible materials, packaging, and several other materials in India, to create lead-free landfills and clean up hazardous sites. TCR Engineering Services undertakes the classification of definitive positive/negative results for Pb using portable XRF instruments.

TCR CAPABILITY:

TCR’s XRF instrument can detect the presence of lead in paints & coatings, as well as in oils & liquids. The tests are done in-situ and it can help in establishing area contamination boundaries and depth profiles, including assisting in site investigations, delineation and contamination patterns.

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